4ce8b626-aaaa-4621-bed3-e70ea756bcfc urn:uuid eng UTF-8 nonGeographicDataset nonGeographicDataset 2025-11-17T07:56:12 creation ISO 19115 2016 Trace elements concentrations measured in sediment leachates from samples collected during the IN2017-V01 voyage of the RV Investigator 4ce8b626-aaaa-4621-bed3-e70ea756bcfc Sediment cores were collected from the East Antarctic margin, aboard the Australian Marine National Facility R/V Investigator, during the IN2017_V01 voyage from January 14th to March 5th 2017 (Armand et al., 2018). This marine geoscience expedition, named the “Sabrina Sea Floor Survey”, focused notably on studying the interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles. The cores were collected using a multi-corer (MC), were sliced every centimetre, wrapped up in plastic bags, and stored in the fridge. Back at the home laboratory (IMAS, UTAS, Hobart, Australia), sediment samples were dried in an oven at 40°C. Three hundred mg of dry sediment was then homogenised and vortexed for 10-sec with 12 mL of a reductive solution of 0.005M hydroxylamine hydrochloride (HH) / 1.5% Acetic Acid (AA) / 0.001M Na-EDTA / 0.033M NaOH, at pH 4 (Huang et al., 2021). The leach mixture was then centrifuged, and 6 mL of the supernatant solution was collected into a Teflon vial. This solution was taken to dryness, oxidized with 1 mL HNO3 + 100 µL H2O2, and redissolved in 4 mL of 7.5M HNO3. A 0.5 mL aliquot was separated from the 4 mL solution for trace metal analysis by Sector Field Inductively Coupled Mass Spectrometry (SF-ICP-MS, Thermo Fisher Scientific, Bremen, Germany) at the Central Science Laboratory (UTAS, Hobart, Australia). Indium was added as internal standard (In, 100 ppb). 88Sr, 89Y, 95Mo, 107Ag, 109Ag, 111Cd, 133Cs, 137Ba, 146Nd, 169Tm, 171Yb, 185Re, 187Re, 205Tl, 208Pb, 232Th, 238U, 23Na, 24Mg, 27Al, 31P, 32S, 42Ca, 47Ti, 51V, 52Cr, 55Mn, 56Fe, 59Co, 60Ni, 63Cu and 66Zn were analysed using multiple spectral resolutions. Element quantification was performed via external calibration using multi-element calibration solutions (MISA suite, QCD Analysts, Spring Lake, NJ, USA). Raw intensities were blank and dilution corrected. References Armand, L. K., O’Brien, P. E., Armbrecht, L., Baker, H., Caburlotto, A., Connell, T., … Young, A. (2018). Interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles (IN2017-V01): Post-survey report. ANU Research Publications, (March). https://doi.org/http://dx.doi.org/10.4225/13/5acea64c48693 Huang, H., Gutjahr, M., Kuhn, G., Hathorne, E. C., and Eisenhauer, A. (2021). Efficient Extraction of Past Seawater Pb and Nd Isotope Signatures From Southern Ocean Sediments. Geochemistry, Geophysics, Geosystems, 22(3), 1–22. https://doi.org/10.1029/2020GC009287 {"type": "Polygon", "coordinates": [[[115.0, -65.0], [120.0, -65.0], [120.0, -64.0], [115.0, -64.0], [115.0, -65.0]]]} 115.0 120.0 -65.0 -64.0 AMD AMD/AU CEOS CONTINENT > ANTARCTICA > WILKES LAND EARTH SCIENCE > OCEANS > MARINE SEDIMENTS EARTH SCIENCE > OCEANS > MARINE SEDIMENTS > SEDIMENT CHEMISTRY EARTH SCIENCE > OCEANS > MARINE SEDIMENTS > SEDIMENT COMPOSITION EARTH SCIENCE > OCEANS > OCEAN CHEMISTRY > TRACE ELEMENTS GEOGRAPHIC REGION > POLAR LABORATORY OCEAN > SOUTHERN OCEAN SEDIMENT LEACH GET DATA > DIRECT DOWNLOAD documentDigital Download the dataset. HTML PROJECT HOME PAGE documentDigital Public information for AAS project AAS_4419 HTML VIEW RELATED INFORMATION documentDigital Citation reference for this metadata record and dataset. HTML Creative Commons by Attribution logo documentDigital PNG